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Highly Sensitive and Robust UPLC-MS/MS Quantification of Nitrosamine Impurities in Sartan and Ranitidine Drug Substances

 

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[ APPLICATION NOTE ] High Sensitivity Quantitation of Nitrosamine Genotoxic Impurities: LC-MS Analysis of Ranitidine Drug Product using the Waters ACQUITY UPLC I-Class/Xevo TQ-XS Tandem Quadrupole Mass Spectrometer Mary Trudeau Lame and Lindsay Hatch Waters Corporation, Milford, MA, USA APPLICATION…
Klíčová slova
ndma, ndmaranitidine, ranitidinenitrosamine, nitrosaminedrug, drugnmba, nmbablank, blankndba, ndbandea, ndeandipa, ndipaproduct, productarea, areaxevo, xevoneipa, neipauplc, uplcimpurities
[ TECHNOLOGY BRIEF ] Highly Sensitive and Robust UPLC-MS/MS Quantification of Nitrosamine Impurities in Sartan and Ranitidine Drug Substances Lindsay Hatch, Mary Lame, Dave Higton, Paul Rainville, and Gordon Fujimoto Waters Corporation, Milford, MA, USA The Xevo TQ-XS Mass Spectrometer,…
Klíčová slova
nitrosamine, nitrosamineranitidine, ranitidinendma, ndmanmba, nmbaneipa, neipandipa, ndipaimpurities, impuritiesndba, ndbandea, ndeadrug, drugquantification, quantificationblank, blanksix, sixnitrosamines, nitrosaminesrecalls
[ TECHNOLOGY BRIEF ] Reliable HPLC/UV Quantification of Nitrosamine Impurities in Valsartan and Ranitidine Drug Substances Margaret Maziarz and Paul Rainville Waters Corporation, Milford, MA, USA The ACQUITY Arc System with PDA Detector, integrated with an ACQUITY QDa Mass Detector…
Klíčová slova
nitrosamine, nitrosaminevalsartan, valsartanqda, qdaranitidine, ranitidinemin, minloq, loqimpurities, impuritiesndma, ndmaacquity, acquitybrief, briefnmba, nmbaneipa, neipandipa, ndipadrug, drugreliable
APPLICATION NOTE 73814 HRAM LC-MS method for the determination of nitrosamine impurities in drugs Authors: Hao Yang, Thermo Fisher Scientific, San Jose, CA, US Jon Bardsley, Thermo Fisher Scientific, Hemel Hempstead, UK Min Du, Thermo Fisher Scientific, Boston, MA, US…
Klíčová slova
positive, positivenitrosamines, nitrosaminesnitrosamine, nitrosaminendma, ndmaranitidine, ranitidinedrug, drugtsim, tsimexcipient, excipientnmea, nmeandipa, ndipanpyr, npyrnpip, npipimpurities, impuritiestms, tmsndpa
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